TA Instruments

AR1717-0001f

04/09/2012 17:51:48

Sample name	ASW 10 mm from base, 60 mm to top, disk 19 Provil novo least texture REMOVED
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1717
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 17:51:48

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

-4.318	7.957	-0.5426	0.99600	22.4	1680	5.5850	10000	0.4123	26.53	6.9812	698.12	3.383E-3	0.0	1.0	60.996	-13.246	6.365
0.7443	12.35	0.06025	1.9960	22.4	1671	13.2599	10000	0.4100	10.95	16.575	1657.5	3.383E-3	0.0	1.0	61.996	2.2835	9.883
1.492	19.37	0.07700	3.0120	22.4	1684	27.1938	10000	0.4133	4.488	33.992	3399.2	3.384E-3	0.1	1.1	63.012	4.5762	15.50
2.055	23.03	0.08926	3.9960	22.4	1669	40.7696	10000	0.4096	3.148	50.962	5096.2	3.383E-3	0.1	1.1	63.996	6.3055	18.42
3.285	30.83	0.1066	4.9960	22.4	1670	67.5136	10000	0.4098	1.757	84.392	8439.2	3.383E-3	0.1	1.1	64.996	10.079	24.66
4.989	39.48	0.1264	5.9920	22.4	1674	106.6260	10000	0.4109	1.074	133.28	13328	3.384E-3	0.1	1.1	65.992	15.306	31.58
5.619	42.53	0.1321	7.0000	22.4	1681	126.3710	10000	0.4127	0.9296	157.96	15796	3.384E-3	0.1	1.1	67.000	17.238	34.02
7.298	49.12	0.1486	7.9960	22.4	1676	165.2370	10000	0.4113	0.6943	206.55	20655	3.384E-3	0.1	1.1	67.996	22.389	39.30
9.784	57.54	0.1700	8.9960	22.4	1672	223.1880	10000	0.4104	0.5051	278.99	27899	3.384E-3	0.1	1.1	68.996	30.016	46.03
11.99	63.69	0.1883	10.016	22.4	1675	274.7660	10000	0.4111	0.4128	343.46	34346	3.384E-3	0.2	1.2	70.016	36.796	50.95
13.88	69.65	0.1992	11.016	22.4	1671	326.0310	10000	0.4102	0.3445	407.54	40754	3.384E-3	0.2	1.2	71.016	42.577	55.72
15.71	75.12	0.2091	12.000	22.4	1670	377.3690	10000	0.4098	0.2959	471.71	47171	3.384E-3	0.2	1.2	72.000	48.200	60.10
17.43	80.51	0.2165	12.996	22.4	1673	435.0360	10000	0.4107	0.2581	543.80	54380	3.384E-3	0.2	1.2	72.996	53.481	64.41
19.63	86.43	0.2271	13.996	22.4	1666	498.9820	10000	0.4088	0.2230	623.73	62373	3.384E-3	0.2	1.2	73.996	60.231	69.15
22.63	94.60	0.2392	14.996	22.4	1655	594.2410	10000	0.4062	0.1849	742.80	74280	3.384E-3	0.2	1.2	74.996	69.418	75.68
24.87	99.91	0.2489	15.996	22.4	1648	664.2860	10000	0.4046	0.1651	830.36	83036	3.384E-3	0.3	1.3	75.996	76.305	79.93
27.24	105.7	0.2578	17.012	22.4	1656	740.9510	10000	0.4064	0.1483	926.19	92619	3.384E-3	0.3	1.3	77.012	83.559	84.53
30.44	113.7	0.2676	17.996	22.4	1652	855.0660	10000	0.4054	0.1277	1068.8	1.0688E5	3.383E-3	0.3	1.3	77.996	93.384	90.99
32.51	118.8	0.2737	18.996	22.4	1657	931.2280	10000	0.4066	0.1174	1164.0	1.1640E5	3.383E-3	0.3	1.3	78.996	99.751	95.04
35.08	124.3	0.2823	19.996	22.4	1642	1020.5700	10000	0.4029	0.1063	1275.7	1.2757E5	3.384E-3	0.3	1.3	79.996	107.63	99.40
39.15	132.3	0.2959	20.996	22.4	1625	1153.4200	10000	0.3989	0.09287	1441.8	1.4418E5	3.383E-3	0.3	1.3	80.996	120.10	105.8
41.79	137.4	0.3042	22.012	22.4	1625	1242.6500	10000	0.3989	0.08612	1553.3	1.5533E5	3.383E-3	0.4	1.4	82.012	128.22	109.9
44.38	142.8	0.3108	23.036	22.4	1630	1344.1200	10000	0.4001	0.07994	1680.2	1.6802E5	3.384E-3	0.4	1.4	83.036	136.14	114.2
48.02	150.8	0.3184	24.012	22.4	1619	1495.7000	10000	0.3973	0.07116	1869.6	1.8696E5	3.384E-3	0.4	1.4	84.012	147.33	120.7
50.76	155.9	0.3256	25.000	22.4	1622	1597.4800	10000	0.3981	0.06672	1996.9	1.9969E5	3.384E-3	0.4	1.4	85.000	155.74	124.7
53.27	161.3	0.3302	25.996	22.4	1619	1713.1400	10000	0.3973	0.06219	2141.4	2.1414E5	3.383E-3	0.4	1.4	85.996	163.44	129.1
57.04	169.3	0.3369	27.004	22.4	1623	1881.9000	10000	0.3983	0.05660	2352.4	2.3524E5	3.383E-3	0.5	1.5	87.004	174.98	135.5
61.28	174.4	0.3513	27.996	22.4	1611	1996.4900	10000	0.3954	0.05295	2495.6	2.4956E5	3.383E-3	0.5	1.5	87.996	188.02	139.6
63.76	179.6	0.3551	29.012	22.4	1614	2115.9800	10000	0.3960	0.05005	2645.0	2.6450E5	3.383E-3	0.5	1.5	89.012	195.63	143.6
68.45	187.6	0.3650	29.996	22.4	1614	2307.0300	10000	0.3960	0.04587	2883.8	2.8838E5	3.384E-3	0.5	1.5	89.996	209.99	150.0
72.14	192.7	0.3744	30.996	22.4	1609	2433.9500	10000	0.3948	0.04333	3042.4	3.0424E5	3.384E-3	0.5	1.5	90.996	221.32	154.2
74.41	197.8	0.3762	32.000	22.4	1614	2635.9600	10000	0.3960	0.04123	3295.0	3.2950E5	3.384E-3	0.5	1.5	92.000	228.30	158.3
79.14	205.8	0.3845	33.012	22.4	1605	2774.1399	10000	0.3938	0.03788	3467.7	3.4677E5	3.384E-3	0.6	1.6	93.012	242.80	164.7
82.91	211.0	0.3930	33.996	22.4	1595	2912.4600	10000	0.3916	0.03584	3640.6	3.6406E5	3.384E-3	0.6	1.6	93.996	254.36	168.8
87.02	218.6	0.3981	35.012	22.4	1581	3128.4500	10000	0.3879	0.03308	3910.6	3.9106E5	3.383E-3	0.6	1.6	95.012	266.96	174.9
90.41	223.9	0.4038	35.996	22.4	1587	3278.9399	10000	0.3896	0.03166	4098.7	4.0987E5	3.383E-3	0.6	1.6	95.996	277.37	179.1
95.30	229.1	0.4160	36.996	22.4	1582	3435.0701	10000	0.3883	0.03015	4293.8	4.2938E5	3.383E-3	0.6	1.6	96.996	292.36	183.3
98.84	236.6	0.4177	37.996	22.4	1576	3658.4600	10000	0.3867	0.02814	4573.1	4.5731E5	3.383E-3	0.6	1.6	97.996	303.22	189.3
102.0	241.8	0.4218	38.996	22.4	1577	3822.6799	10000	0.3871	0.02697	4778.4	4.7784E5	3.383E-3	0.6	1.6	98.996	312.94	193.5
108.4	249.6	0.4342	39.996	22.4	1548	4068.2500	10000	0.3800	0.02486	5085.3	5.0853E5	3.383E-3	0.7	1.7	99.996	332.47	199.7
111.1	254.6	0.4362	41.012	22.4	1565	4232.3198	10000	0.3841	0.02414	5290.4	5.2904E5	3.384E-3	0.7	1.7	101.012	340.72	203.7
114.8	259.8	0.4418	42.008	22.4	1550	4498.8101	10000	0.3804	0.02296	5623.5	5.6235E5	3.383E-3	0.7	1.7	102.008	352.16	207.9
121.0	267.6	0.4521	42.996	22.4	1554	4674.4600	10000	0.3814	0.02170	5843.1	5.8431E5	3.384E-3	0.7	1.7	102.996	371.17	214.1
124.4	272.7	0.4562	44.000	22.4	1558	4851.0498	10000	0.3824	0.02096	6063.8	6.0638E5	3.383E-3	0.7	1.7	104.000	381.64	218.1
130.2	280.3	0.4644	45.008	22.4	1540	5128.5498	10000	0.3780	0.01960	6410.7	6.4107E5	3.384E-3	0.8	1.8	105.008	399.37	224.3
134.5	285.5	0.4712	45.996	22.4	1528	5317.8799	10000	0.3751	0.01875	6647.4	6.6474E5	3.384E-3	0.8	1.8	105.996	412.73	228.4
140.4	293.1	0.4791	46.996	22.4	1547	5601.8701	10000	0.3796	0.01800	7002.3	7.0023E5	3.384E-3	0.8	1.8	106.996	430.80	234.5
144.5	298.1	0.4848	47.996	22.4	1535	5797.7202	10000	0.3768	0.01727	7247.2	7.2472E5	3.384E-3	0.8	1.8	107.996	443.40	238.5
147.7	303.3	0.4870	49.016	22.4	1527	5999.3398	10000	0.3747	0.01659	7499.2	7.4992E5	3.383E-3	0.8	1.8	109.016	453.17	242.7
151.9	311.0	0.4884	49.996	22.4	1523	6301.9800	10000	0.3737	0.01575	7877.5	7.8775E5	3.384E-3	0.8	1.8	109.996	465.91	248.8
158.1	316.0	0.5002	51.000	22.4	1514	6510.2002	10000	0.3717	0.01517	8137.8	8.1378E5	3.384E-3	0.9	1.9	111.000	484.96	252.8
163.4	323.8	0.5046	52.016	22.4	1512	6831.7100	10000	0.3711	0.01442	8539.6	8.5396E5	3.384E-3	0.9	1.9	112.016	501.23	259.0
168.9	328.9	0.5136	53.000	22.4	1499	7049.9302	10000	0.3678	0.01386	8812.4	8.8124E5	3.383E-3	0.9	1.9	113.000	518.13	263.1
174.2	336.4	0.5177	53.996	22.4	1495	7384.6099	10000	0.3670	0.01321	9230.8	9.2308E5	3.383E-3	0.9	1.9	113.996	534.34	269.1
176.1	341.6	0.5154	54.996	22.4	1495	7600.9199	10000	0.3668	0.01281	9501.2	9.5012E5	3.384E-3	0.9	1.9	114.996	540.12	273.3
180.5	346.7	0.5206	56.012	22.4	1500	7942.8101	10000	0.3682	0.01248	9928.5	9.9285E5	3.384E-3	0.9	1.9	116.012	553.73	277.3
189.1	354.2	0.5339	57.012	22.4	1502	8168.3999	10000	0.3687	0.01197	10211	1.0211E6	3.384E-3	1.0	2.0	117.012	580.21	283.4
191.1	359.3	0.5317	57.996	22.4	1503	8408.9600	10000	0.3689	0.01164	10511	1.0511E6	3.384E-3	1.0	2.0	117.996	586.16	287.5
198.0	367.0	0.5396	58.996	22.4	1475	8767.3896	10000	0.3620	0.01095	10959	1.0959E6	3.384E-3	1.0	2.0	118.996	607.47	293.6
200.9	372.0	0.5401	60.000	22.4	1469	9006.8398	10000	0.3605	0.01062	11259	1.1259E6	3.384E-3	1.0	2.0	120.000	616.36	297.6

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

203.3	375.0	0.5422	0.99600	22.4	1509	285.3690	10000	0.3703	0.01073	356.71	35671	3.384E-3	0.0	2.0	121.996	623.77	300.0
204.0	375.0	0.5441	1.9960	22.4	1471	535.4450	10000	0.3609	0.01046	669.31	66931	3.384E-3	0.0	2.0	122.996	625.96	300.0
210.5	375.0	0.5615	3.0120	22.4	1452	912.4530	10000	0.3565	0.01033	1140.6	1.1406E5	3.383E-3	0.1	2.1	124.012	645.95	300.0
210.1	375.0	0.5602	4.0000	22.4	1457	1163.9399	10000	0.3575	0.01036	1454.9	1.4549E5	3.383E-3	0.1	2.1	125.000	644.52	300.0
209.1	375.0	0.5577	5.0000	22.4	1481	1416.2400	10000	0.3636	0.01053	1770.3	1.7703E5	3.384E-3	0.1	2.1	126.000	641.57	300.0
206.9	375.0	0.5519	6.0000	22.4	1453	1794.5000	10000	0.3567	0.01033	2243.1	2.2431E5	3.384E-3	0.1	2.1	127.000	634.89	300.0
211.0	375.0	0.5627	6.9960	22.4	1451	2045.3800	10000	0.3561	0.01032	2556.7	2.5567E5	3.384E-3	0.1	2.1	127.996	647.38	300.0
206.1	375.0	0.5496	7.9960	22.4	1471	2420.4299	10000	0.3611	0.01046	3025.5	3.0255E5	3.384E-3	0.1	2.1	128.996	632.26	300.0
209.7	375.0	0.5591	8.9960	22.4	1438	2671.7300	10000	0.3530	0.01023	3339.7	3.3397E5	3.383E-3	0.1	2.2	129.996	643.27	300.0
209.1	375.0	0.5577	10.008	22.4	1482	2925.2900	10000	0.3638	0.01054	3656.6	3.6566E5	3.383E-3	0.2	2.2	131.008	641.60	300.0
207.4	375.0	0.5532	11.012	22.4	1468	3300.1699	10000	0.3603	0.01044	4125.2	4.1252E5	3.384E-3	0.2	2.2	132.012	636.40	300.0
207.3	375.0	0.5528	11.996	22.4	1464	3551.4800	10000	0.3593	0.01041	4439.4	4.4394E5	3.384E-3	0.2	2.2	132.996	635.94	300.0
205.9	375.0	0.5491	12.996	22.4	1476	3929.8899	10000	0.3622	0.01049	4912.4	4.9124E5	3.384E-3	0.2	2.2	133.996	631.67	300.0
207.9	375.0	0.5543	13.996	22.4	1452	4179.6802	10000	0.3565	0.01033	5224.6	5.2246E5	3.383E-3	0.2	2.2	134.996	637.78	300.0
206.0	375.0	0.5494	14.996	22.4	1485	4431.6602	10000	0.3644	0.01056	5539.6	5.5396E5	3.384E-3	0.2	2.3	135.996	632.05	300.0
205.7	375.0	0.5486	16.000	22.4	1466	4809.3501	10000	0.3597	0.01042	6011.7	6.0117E5	3.383E-3	0.3	2.3	137.000	631.18	300.0
206.7	375.0	0.5513	17.000	22.4	1470	5065.6899	10000	0.3607	0.01045	6332.1	6.3321E5	3.384E-3	0.3	2.3	138.000	634.24	300.0
203.2	375.0	0.5419	17.996	22.4	1495	5310.6699	10000	0.3668	0.01063	6638.3	6.6383E5	3.383E-3	0.3	2.3	138.996	623.46	300.0
201.3	375.0	0.5368	18.996	22.4	1492	5687.7100	10000	0.3662	0.01061	7109.6	7.1096E5	3.383E-3	0.3	2.3	139.996	617.64	300.0
210.1	375.0	0.5603	19.996	22.4	1423	5939.0298	10000	0.3494	0.01012	7423.8	7.4238E5	3.383E-3	0.3	2.3	140.996	644.68	300.0
207.9	375.0	0.5544	20.996	22.4	1450	6316.0498	10000	0.3559	0.01031	7895.1	7.8951E5	3.383E-3	0.3	2.4	141.996	637.85	300.0
209.9	375.0	0.5596	21.996	22.4	1450	6567.3398	10000	0.3559	0.01031	8209.2	8.2092E5	3.383E-3	0.4	2.4	142.996	643.89	300.0
205.7	375.0	0.5485	23.016	22.4	1464	6818.5298	10000	0.3593	0.01041	8523.2	8.5232E5	3.383E-3	0.4	2.4	144.016	631.03	300.0
204.7	375.0	0.5459	23.996	22.4	1454	7197.0898	10000	0.3569	0.01034	8996.4	8.9964E5	3.383E-3	0.4	2.4	144.996	628.01	300.0
205.7	375.0	0.5485	24.996	22.4	1469	7451.8398	10000	0.3605	0.01045	9314.8	9.3148E5	3.384E-3	0.4	2.4	145.996	631.06	300.0
203.7	375.0	0.5432	26.004	22.4	1496	7827.6802	10000	0.3672	0.01064	9784.6	9.7846E5	3.383E-3	0.4	2.5	147.004	624.96	300.0
207.8	375.0	0.5540	26.996	22.4	1460	8076.0698	10000	0.3583	0.01038	10095	1.0095E6	3.384E-3	0.4	2.5	147.996	637.38	300.0
208.2	375.0	0.5551	27.992	22.4	1432	8328.0098	10000	0.3514	0.01018	10410	1.0410E6	3.384E-3	0.5	2.5	148.992	638.70	300.0
208.0	375.0	0.5547	28.996	22.4	1432	8703.9902	10000	0.3514	0.01018	10880	1.0880E6	3.384E-3	0.5	2.5	149.996	638.24	300.0
209.7	375.0	0.5593	29.996	22.4	1439	8956.1396	10000	0.3532	0.01023	11195	1.1195E6	3.384E-3	0.5	2.5	150.996	643.50	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

202.6	370.5	0.5468	1.0000	22.4	1477	293.3990	10000	0.3626	0.01076	366.75	36675	3.384E-3	0.0	2.5	152.000	621.62	296.4
195.0	365.5	0.5335	2.0000	22.4	1474	531.4470	10000	0.3618	0.01103	664.31	66431	3.383E-3	0.0	2.6	153.000	598.20	292.4
192.3	357.9	0.5373	3.0160	22.4	1449	888.3880	10000	0.3557	0.01131	1110.5	1.1105E5	3.384E-3	0.1	2.6	154.016	589.92	286.3
184.7	352.7	0.5236	4.0000	22.4	1533	1126.2200	10000	0.3762	0.01232	1407.8	1.4078E5	3.384E-3	0.1	2.6	155.000	566.64	282.2
181.3	347.7	0.5215	5.0000	22.4	1463	1353.4000	10000	0.3591	0.01211	1691.8	1.6918E5	3.384E-3	0.1	2.6	156.000	556.27	278.1
179.9	340.1	0.5289	6.0160	22.4	1486	1689.9100	10000	0.3648	0.01285	2112.4	2.1124E5	3.384E-3	0.1	2.6	157.016	551.80	272.0
178.2	334.9	0.5321	7.0040	22.4	1476	1915.0200	10000	0.3624	0.01316	2393.8	2.3938E5	3.384E-3	0.1	2.6	158.004	546.74	267.9
169.2	327.4	0.5168	8.0000	22.4	1485	2236.0500	10000	0.3646	0.01386	2795.1	2.7951E5	3.384E-3	0.1	2.7	159.000	519.02	261.9
163.9	322.3	0.5084	9.0000	22.4	1525	2447.3000	10000	0.3743	0.01468	3059.1	3.0591E5	3.384E-3	0.2	2.7	160.000	502.70	257.8
161.2	314.5	0.5126	10.000	22.4	1501	2766.5500	10000	0.3684	0.01517	3458.2	3.4582E5	3.384E-3	0.2	2.7	161.000	494.65	251.6
155.2	309.5	0.5014	11.000	22.4	1519	2968.5200	10000	0.3729	0.01586	3710.7	3.7107E5	3.384E-3	0.2	2.7	162.000	476.08	247.6
147.0	304.5	0.4829	12.000	22.4	1550	3174.5701	10000	0.3804	0.01672	3968.2	3.9682E5	3.384E-3	0.2	2.7	163.000	451.07	243.6
143.8	296.7	0.4846	13.000	22.4	1520	3470.9299	10000	0.3731	0.01727	4338.7	4.3387E5	3.383E-3	0.2	2.7	164.000	441.16	237.4
138.5	291.5	0.4752	14.000	22.4	1542	3663.2100	10000	0.3784	0.01814	4579.0	4.5790E5	3.383E-3	0.2	2.8	165.000	424.99	233.2
133.9	283.9	0.4715	15.000	22.4	1537	3942.9900	10000	0.3772	0.01906	4928.7	4.9287E5	3.383E-3	0.3	2.8	166.000	410.73	227.2
130.5	278.8	0.4681	16.000	22.4	1528	4130.7002	10000	0.3751	0.01966	5163.4	5.1634E5	3.383E-3	0.3	2.8	167.000	400.39	223.0
122.5	271.2	0.4516	16.992	22.4	1545	4400.7598	10000	0.3792	0.02101	5501.0	5.5010E5	3.384E-3	0.3	2.8	167.992	375.73	216.9
119.6	266.1	0.4495	18.000	22.4	1571	4575.2700	10000	0.3855	0.02218	5719.1	5.7191E5	3.384E-3	0.3	2.8	169.000	366.95	212.9
116.8	261.0	0.4475	19.000	22.4	1555	4750.1099	10000	0.3816	0.02283	5937.6	5.9376E5	3.383E-3	0.3	2.8	170.000	358.30	208.8
111.1	253.2	0.4387	20.000	22.4	1554	5007.1602	10000	0.3814	0.02425	6259.0	6.2590E5	3.384E-3	0.3	2.9	171.000	340.71	202.5
107.8	248.1	0.4345	21.000	22.4	1544	5168.9800	10000	0.3790	0.02508	6461.2	6.4612E5	3.384E-3	0.4	2.9	172.000	330.80	198.5
102.2	240.4	0.4252	21.996	22.4	1566	5413.6899	10000	0.3843	0.02709	6767.1	6.7671E5	3.384E-3	0.4	2.9	172.996	313.60	192.3
98.66	235.1	0.4196	23.000	22.4	1570	5575.3999	10000	0.3853	0.02840	6969.3	6.9693E5	3.384E-3	0.4	2.9	174.000	302.70	188.1
95.58	230.0	0.4155	23.996	22.4	1588	5726.1001	10000	0.3898	0.03001	7157.6	7.1576E5	3.384E-3	0.4	2.9	174.996	293.23	184.0
89.45	222.3	0.4023	25.000	22.4	1586	5950.4199	10000	0.3891	0.03207	7438.0	7.4380E5	3.384E-3	0.4	2.9	176.000	274.44	177.9
86.96	217.1	0.4006	26.000	22.4	1581	6100.2700	10000	0.3881	0.03357	7625.3	7.6253E5	3.384E-3	0.4	3.0	177.000	266.80	173.6
81.64	209.5	0.3897	26.996	22.4	1587	6306.4902	10000	0.3896	0.03617	7883.1	7.8831E5	3.384E-3	0.4	3.0	177.996	250.47	167.6
79.29	204.3	0.3880	28.000	22.4	1590	6443.9502	10000	0.3902	0.03807	8054.9	8.0549E5	3.384E-3	0.5	3.0	179.000	243.26	163.5
75.22	199.1	0.3779	28.996	22.4	1614	6581.9502	10000	0.3960	0.04072	8227.4	8.2274E5	3.383E-3	0.5	3.0	179.996	230.78	159.3
70.68	191.3	0.3695	30.012	22.4	1602	6774.8501	10000	0.3932	0.04379	8468.6	8.4686E5	3.384E-3	0.5	3.0	181.012	216.84	153.0
67.56	186.1	0.3629	30.992	22.4	1607	6900.0601	10000	0.3944	0.04638	8625.1	8.6251E5	3.383E-3	0.5	3.0	181.992	207.26	148.9
65.54	180.9	0.3623	32.000	22.4	1609	7025.1802	10000	0.3950	0.04920	8781.5	8.7815E5	3.383E-3	0.5	3.1	183.000	201.06	144.7
59.97	173.1	0.3464	32.996	22.4	1603	7199.7998	10000	0.3934	0.05349	8999.8	8.9998E5	3.384E-3	0.5	3.1	183.996	183.99	138.5
57.40	168.0	0.3417	33.996	22.4	1619	7312.0601	10000	0.3973	0.05734	9140.1	9.1401E5	3.383E-3	0.6	3.1	184.996	176.11	134.4
52.76	160.1	0.3296	35.000	22.4	1629	7480.5400	10000	0.3997	0.06355	9350.7	9.3507E5	3.383E-3	0.6	3.1	186.000	161.88	128.1
49.55	154.7	0.3203	35.996	22.4	1619	7587.1099	10000	0.3975	0.06766	9483.9	9.4839E5	3.383E-3	0.6	3.1	186.996	152.02	123.8
46.58	149.6	0.3113	36.996	22.4	1628	7686.1099	10000	0.3995	0.07269	9607.6	9.6076E5	3.384E-3	0.6	3.1	187.996	142.91	119.7
43.20	141.7	0.3049	38.000	22.4	1619	7835.2500	10000	0.3975	0.08065	9794.1	9.7941E5	3.384E-3	0.6	3.2	189.000	132.55	113.4
40.47	136.2	0.2972	38.996	22.4	1625	7934.6699	10000	0.3989	0.08767	9918.3	9.9183E5	3.384E-3	0.6	3.2	189.996	124.16	108.9
38.31	130.9	0.2926	40.000	22.4	1633	8021.7900	10000	0.4007	0.09524	10027	1.0027E6	3.383E-3	0.7	3.2	191.000	117.55	104.7
34.14	123.0	0.2777	40.996	22.4	1643	8152.4302	10000	0.4031	0.1086	10191	1.0191E6	3.384E-3	0.7	3.2	191.996	104.74	98.37
31.50	117.4	0.2684	42.000	22.4	1645	8241.2695	10000	0.4038	0.1194	10302	1.0302E6	3.384E-3	0.7	3.2	193.000	96.647	93.89
29.91	112.1	0.2668	43.004	22.4	1625	8314.0703	10000	0.3989	0.1293	10393	1.0393E6	3.383E-3	0.7	3.2	194.004	91.769	89.69
27.23	104.1	0.2615	43.996	22.4	1656	8426.2100	10000	0.4064	0.1527	10533	1.0533E6	3.384E-3	0.7	3.2	194.996	83.545	83.30
24.07	98.43	0.2445	45.000	22.4	1650	8500.1699	10000	0.4050	0.1703	10625	1.0625E6	3.384E-3	0.8	3.3	196.000	73.844	78.75
22.08	93.18	0.2369	45.996	22.4	1648	8562.2695	10000	0.4046	0.1899	10703	1.0703E6	3.384E-3	0.8	3.3	196.996	67.730	74.54
19.67	87.88	0.2238	47.000	22.4	1662	8624.4902	10000	0.4080	0.2153	10781	1.0781E6	3.383E-3	0.8	3.3	198.000	60.335	70.30
17.60	82.25	0.2140	48.000	22.4	1662	8686.0000	10000	0.4078	0.2456	10858	1.0858E6	3.384E-3	0.8	3.3	199.000	53.988	65.80
14.71	73.99	0.1989	49.000	22.4	1676	8766.2695	10000	0.4113	0.3061	10958	1.0958E6	3.384E-3	0.8	3.3	200.000	45.137	59.19
13.04	68.63	0.1901	50.000	22.4	1658	8815.6104	10000	0.4070	0.3521	11020	1.1020E6	3.384E-3	0.8	3.4	201.000	40.015	54.90
11.11	62.83	0.1767	50.996	22.4	1652	8864.7803	10000	0.4056	0.4186	11081	1.1081E6	3.384E-3	0.8	3.4	201.996	34.070	50.26
9.454	56.88	0.1662	52.004	22.4	1664	8907.9697	10000	0.4084	0.5143	11135	1.1135E6	3.384E-3	0.9	3.4	203.004	29.005	45.51
7.531	48.79	0.1544	52.996	22.4	1669	8962.9102	10000	0.4096	0.7012	11204	1.1204E6	3.384E-3	0.9	3.4	203.996	23.104	39.03
5.951	42.60	0.1397	54.000	22.4	1670	8999.3203	10000	0.4098	0.9201	11249	1.1249E6	3.384E-3	0.9	3.4	205.000	18.256	34.08
4.379	36.07	0.1214	54.992	22.4	1669	9029.6602	10000	0.4096	1.283	11287	1.1287E6	3.384E-3	0.9	3.4	205.992	13.436	28.86
3.300	30.44	0.1084	55.996	22.4	1669	9053.6104	10000	0.4096	1.801	11317	1.1317E6	3.384E-3	0.9	3.4	206.996	10.124	24.35
2.794	27.23	0.1026	56.996	22.4	1672	9065.4600	10000	0.4104	2.256	11332	1.1332E6	3.384E-3	0.9	3.5	207.996	8.5715	21.78
1.606	19.48	0.08247	57.996	22.4	1659	9088.4102	10000	0.4072	4.374	11361	1.1361E6	3.384E-3	1.0	3.5	208.996	4.9276	15.58
0.8100	12.69	0.06383	58.992	22.4	1665	9099.7998	10000	0.4086	10.34	11375	1.1375E6	3.383E-3	1.0	3.5	209.992	2.4850	10.15
0.4652	8.754	0.05315	59.996	22.4	1678	9104.7900	10000	0.4119	21.90	11381	1.1381E6	3.383E-3	1.0	3.5	210.996	1.4273	7.003

